HCID 59252318, compound → HCID 59252304, compound

HRID 2265904Notes

Reaction equation

HRID 2265904 reaction equation
[CH3:1][O:2][C:3](=[O:15])[CH:4]=[C:5]1[CH2:10][CH2:9][CH:8]([O:11][CH:12]([CH3:14])[CH3:13])[CH2:7][CH2:6]1>C(OC(=O)C)C.[Pd]>[CH3:1][O:2][C:3](=[O:15])[CH2:4][CH:5]1[CH2:10][CH2:9][CH:8]([O:11][CH:12]([CH3:13])[CH3:14])[CH2:7][CH2:6]1

Participants

4

Reactant 1

HCID 59252318HCID 59252318, compound

Product 1

HCID 59252304HCID 59252304, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8857Ethyl AcetateSolvent

Procedure

Prepared from (4-isopropoxy-cyclohexylidene)-acetic acid methyl ester (0.500 g, 2.36 mmol) by hydrogenation 16 hours at room temperature using Pd/C (10%) (50 mg) in ethylacetate (15 ml). cis/trans mixture. MS (m/e): 215.4 (M+H+).

Sources & evidence

ORD record
ord-b60c6227eaf94741ba899e0e35166904
Source dataset
uspto-grants-2010_12
Patent number
US07858630B2

Reaction notes

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