HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxypropyne → HCID 86625535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxypropyne | HCID 69393 | — |
| Reactant | HCID 59598164 | HCID 59598164 | — |
| Product | HCID 86625535 | HCID 86625535 | 22% |
Reaction Steps
2-Chloro-N-methoxy-N-methyl-6-trifluoromethyl-nicotinamide (1000 mg, 3.72 mmol) was reacted with 3-methoxy-propyne (0.345 ml, 4.09 mmol) to give N-methoxy-2-(3-methoxy-prop-1-ynyl)-N-methyl-6-trifluoromethyl-nicotinamide (247 mg, 22%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858621B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-8e7313c0ea594e1083177f8ede04df43 |
| Source note | uspto-grants-2010_12 |