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HRID2267068

反应详情

EQUATION

反应方程式

HRID 2267068 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)c1ccc(O)c(C)c1O
HCID592139

1-(2,4-Dihydroxy-3-methylphenyl)ethanone

C9H10O3

结构：N#Cc1ccnc(Sc2cccc(CO)c2)c1
HCID57355460

2-{[3-(Hydroxymethyl)phenyl]sulfanyl}pyridine-4-carbonitrile

C13H10N2OS

PRODUCTS

生成物

1
结构：CC(=O)c1ccc(OCc2cccc(Sc3cc(C#N)ccn3)c2)c(C)c1O
HCID68537769

未命名化合物

收率 52%

PROCEDURE

实验过程

Using the method of Preparation 166 using 2-(3-(hydroxymethyl)phenylthio) isonicotinonitrile (1.46 g, 6.02 mmol) and 1-(2,4-dihydroxy-3-methylphenyl)ethanone (1.00 g, 6.02 mmol) affords the title compound (1.22 g, 52%). MS (APCI-neg) m/z (rel intensity): 389 (M−H, 100%).