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HRID2267070

反应详情

EQUATION

反应方程式

HRID 2267070 的结构方程式

REACTANTS

反应物

2
结构：CCc1c(O)ccc(C(C)=O)c1O
HCID21287021

1-(3-Ethyl-2,4-dihydroxyphenyl)ethan-1-one

C10H12O3

结构：N#Cc1ccnc(Sc2cccc(CO)c2)c1
HCID57355460

2-{[3-(Hydroxymethyl)phenyl]sulfanyl}pyridine-4-carbonitrile

C13H10N2OS

PRODUCTS

生成物

1
结构：CCc1c(OCc2cccc(Sc3cc(C#N)ccn3)c2)ccc(C(C)=O)c1O
HCID68535845

未命名化合物

收率 80%

PROCEDURE

实验过程

Using the method of Preparation 166 using 6-(3-(hydroxymethyl)phenylthio) isonicotinonitrile (1.35 g, 5.56 mmol) and 1-(3-ethyl-2,4-dihydroxyphenyl)ethanone (1.00 g, 5.56 mmol) affords the title compound (1.80 g, 80%). MS (APCI-neg) m/z (rel intensity): 403 (M−H, 100%).