HRID2267152

反应详情

EQUATION

反应方程式

HRID 2267152 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

tert-Butyl 4-[1-phenyl-1H-[1,2,3]triazol-4-yl]-1,2,3,6-tetrahydropyridine-1-carboxylate (5 mg) was dissolved in 1 ml of ethanol, a catalytic amount of 20% palladium hydroxide was added and the mixture was vigorously stirred for 30 minutes in a hydrogen atmosphere. The reaction solution was filtered through Celite. The solvent was evaporated from the resulting filtrate to give 5 mg of the title compound as a white solid.

WORKUP

后处理

  1. filtrationThe reaction solution was filtered through Celite
  2. customThe solvent was evaporated from the resulting filtrate