HCID 58945846, compound → HCID 68428331, compound

HRID 2267157Notes

Reaction equation

HRID 2267157 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[C:12]([CH3:13])=[C:11]([C:14]2[CH2:15][CH2:16][N:17](C(OC(C)(C)C)=O)[CH2:18][CH:19]=2)[N:10]=[N:9]1>Cl>[ClH:1].[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[C:12]([CH3:13])=[C:11]([C:14]2[CH2:15][CH2:16][NH:17][CH2:18][CH:19]=2)[N:10]=[N:9]1

Participants

3

Reactant 1

HCID 58945846HCID 58945846, compound

Product 1

HCID 68428331HCID 68428331, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

tert-Butyl 4-[1-(2-chlorophenyl)-5-methyl-1H-[1,2,3]-triazol-4-yl]-1,2,3,6-tetrahydropyridine-1-carboxylate (40 mg) prepared in Example 10 was dissolved in 10% methanolic hydrochloric acid and stirred at room temperature for 3.5 hours and the solvent was evaporated in vacuo to give the title compound as a mixture.

Workup

  1. customthe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-3e2e20a3fc384e499097012d0a1b311e
Source dataset
uspto-grants-2010_12
Patent number
US07858800B2

Reaction notes

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