Hydrochloric Acid → HCID 68430404, compound

HRID 2267158Notes

Reaction equation

HRID 2267158 reaction equation
[C:1]1([N:7]2[C:11]([CH3:12])=[C:10]([C:13]3[CH2:14][CH2:15][N:16](C(OC(C)(C)C)=O)[CH2:17][CH:18]=3)[N:9]=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[ClH:26]>>[ClH:26].[CH3:12][C:11]1[N:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[N:8]=[N:9][C:10]=1[C:13]1[CH2:14][CH2:15][NH:16][CH2:17][CH:18]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 58945818HCID 58945818, compound

Product 1

HCID 68430404HCID 68430404, compound

Procedure

tert-Butyl 4-[1-phenyl-5-methyl-1H-[1,2,3]-triazol-4-yl]-1,2,3,6-tetrahydropyridine-1-carboxylate (7.4 mg) prepared in Example 7 was dissolved in 2.0 ml of 10% methanolic hydrochloric acid solution and stirred at room temperature for 10 minutes. The solvent was evaporated in vacuo to give the title compound as a brown solid crude product.

Workup

  1. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-4701c466f6724c668156cb4e9e79cf8b
Source dataset
uspto-grants-2010_12
Patent number
US07858800B2

Reaction notes

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