HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68428068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58945819 | HCID 58945819 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68428068 | HCID 68428068 | 60.1% |
Reaction Steps
A 4N solution of hydrochloric acid in dioxane (3 ml) was added to 15 mg of tert-butyl 4-[5-methyl-1-(pyridine-3-yl)-1H-[1,2,3]triazol-4-yl]-1,2,3,6-tetrahydropyridine-1-carboxylate, the mixture was stirred at room temperature for 3 hours and the solvent was evaporated in vacuo to give 6 mg of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858800B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-a488d47c01204ead84a4590a9dc731c2 |
| Source note | uspto-grants-2010_12 |