HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 68428295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 44588385 | HCID 44588385 | — |
| Product | HCID 68428295 | HCID 68428295 | — |
Reaction Steps
tert-Butyl 4-[1-(2-fluorophenyl)-1H-[1,2,3]triazol-4-yl]-1,2,3,6-tetrahydropyridine-1-carboxylate (70 mg) prepared in Example 5 was dissolved in 2.0 ml of 4N hydrochloric acid/ethyl acetate solution followed by stirring at room temperature for 30 minutes. The solvent was evaporated in vacuo to give the title compound as a brown crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858800B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-3643f6c821a8416b8860efc85a9782c3 |
| Source note | uspto-grants-2010_12 |