Hydrochloric Acid → HCID 68429818, compound

Participants

Reaction Steps

4N Hydrochloric acid solution in dioxane (10 ml) was added to 150 mg of tert-butyl 4-[1-(2-chlorophenyl)-5-methyl-1H-[1,2,3]-triazol-4-yl]-3-oxopiperazine-1-carboxylate prepared in Example 26, the mixture was stirred at room temperature for 3 hours and the solvent was evaporated in vacuo to give 110 mg of the title compound as a white solid.

Provenance & Evidence