HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58945859, compound → 4-(5-methyl-1-phenyl-1H-[1,2,3]-triazol-4-yl)-3-oxopiperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58945859 | HCID 58945859 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | 4-(5-methyl-1-phenyl-1H-[1,2,3]-triazol-4-yl)-3-oxopiperazine | HCID 68431061 | — |
Reaction Steps
4N hydrochloric acid/dioxane solution (10 ml) was added to tert-butyl 4-(5-methyl-1-phenyl-1H-[1,2,3]triazol-4-yl)-3-oxopiperazine-1-carboxylate prepared in Example 29 followed by stirring at room temperature for 3 hours and the solvent was evaporated in vacuo to give 60 mg of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858800B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-fa1d7e35feb144059cfd7cab5ef9477f |
| Source note | uspto-grants-2010_12 |