TIBA cyclohexane → 2,3,5-Triiodobenzoic acid

Participants

Reaction Steps

39.1 mL of TIBA/cyclohexane solution (113 g/L) were mixed with 2.8 mL of MAO/toluene solution to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 h at room temperature and transferred into a 50 mL Schlenk flask containing 21.1 mg of C1. This solution was diluted with 6.78 mL of cyclohexane to give an orange solution of concentration 100 gTOT/L and 0.99 gmetallocene/L.

Provenance & Evidence