HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 60204495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 60204494 | HCID 60204494 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 60204495 | HCID 60204495 | — |
Reaction Steps
A solution of 15 mg (0.024 mmol) of tert-Butyl 2-(3-{4-(5-chlorothiophen-2-yl)-2-[2-(5,5-dimethyl-2,4-dioxoimidazolidin-1-yl)ethylamino]pyrimidin-5-yl}phenylamino)-2-oxoethyl(methyl)carbamate in 1 mL of 1,4-dioxane was treated with 2 mL of a 4 M solution of HCl in 1,4-dioxane and stirred 1 h at rt, then concentrated in vacuo to give the desired product as the hydrochloride salt. MS (M+H)+ 528.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858785B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-d7b64e7b3d994239b834f5d51d5a4b90 |
| Source note | uspto-grants-2010_12 |