HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68605009, compound → HCID 68606635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68605009 | HCID 68605009 | — |
| Reactant | HCID 86619279 | HCID 86619279 | — |
| Product | HCID 68606635 | HCID 68606635 | — |
Reaction Steps
A method similar to that used for the preparation of (107a) was used except that methyl-L-methionine hydrochloride (214 mg) was used instead of methyl-L-valinate hydrochloride to afford the desired product (300 mg). 1H NMR (300 MHz, CDCl3) δ 1.178 (t, 3H, J=7 Hz), 1.93 (m, 2H), 2.02 (s, 3H), 2.51 (m, 2H), 3.53 (s, 2H), 4.38 (m, 1H), 7.07 (m, 3H), 8.54 (d, 1H, J=8 Hz). LC/MS: 2.28 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858776B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-0de07464356b4642b3c53976a775e689 |
| Source note | uspto-grants-2010_12 |