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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2267666Generated: October 30, 2026

HCID 68605009, compound → HCID 68606635, compound

https://huagongshe.com/reaction/2267666

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68605009HCID 68605009—
ReactantHCID 86619279HCID 86619279—
ProductHCID 68606635HCID 68606635—

Reaction Steps

A method similar to that used for the preparation of (107a) was used except that methyl-L-methionine hydrochloride (214 mg) was used instead of methyl-L-valinate hydrochloride to afford the desired product (300 mg). 1H NMR (300 MHz, CDCl3) δ 1.178 (t, 3H, J=7 Hz), 1.93 (m, 2H), 2.02 (s, 3H), 2.51 (m, 2H), 3.53 (s, 2H), 4.38 (m, 1H), 7.07 (m, 3H), 8.54 (d, 1H, J=8 Hz). LC/MS: 2.28 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07858776B2
Source datasetuspto-grants-2010_12
ORD IDord-0de07464356b4642b3c53976a775e689
Source noteuspto-grants-2010_12