Hydrochloric Acid → HCID 66841786, compound

HRID 2267693Notes

Reaction equation

HRID 2267693 reaction equation
C(OC(=O)[NH:7][CH:8]1[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][N:16]2[CH2:21][CH2:20][CH:19]([OH:22])[CH2:18][CH2:17]2)[CH2:10][CH2:9]1)(C)(C)C.[ClH:24]>O1CCOCC1>[ClH:24].[ClH:24].[ClH:24].[NH2:7][CH:8]1[CH2:9][CH2:10][N:11]([CH2:14][CH2:15][N:16]2[CH2:17][CH2:18][CH:19]([OH:22])[CH2:20][CH2:21]2)[CH2:12][CH2:13]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 66841294HCID 66841294, compound

Product 1

HCID 66841786HCID 66841786, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Ester 23 (2.2 g, 6.72 mmol) is dissolved in 4M HCl in dioxane at 0° C. and stirred at room temperature for 3 hours. After evaporation of the solvent the product is dried at high vacuum.

Workup

  1. customAfter evaporation of the solvent the product
  2. customis dried at high vacuum

Sources & evidence

ORD record
ord-ffb38c11b0fd4dd3934ecced876fba60
Source dataset
uspto-grants-2010_12
Patent number
US07858781B2

Reaction notes

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