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HRID2267695

反应详情

EQUATION

反应方程式

HRID 2267695 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)NC1CCN(CCN2C3CCC2CC(O)C3)CC1
HCID66841981

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.Cl.NC1CCN(CCN2C3CCC2CC(O)C3)CC1
HCID66841574

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

Ester 26 (4.5 g, 12.73 mmol) is dissolved in 4M HCl in dioxane at 0° C. and stirred at room temperature for 3 hours. After evaporation of the solvent the product is dried at high vacuum.

WORKUP

后处理

  1. customAfter evaporation of the solvent the product
  2. customis dried at high vacuum