HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylhydrazine → HCID 18606553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | 1-Benzyl-3-methyl-4-piperidone | HCID 560965 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18606553 | HCID 18606553 | — |
Reaction Steps
N,N-dimethylhydrazine (3 ml, 39.3 mmol) and 1-benzyl-3-methyl-piperidin-4-one (4 g, 19.7 mmol) are dissolved in 50 ml of ethanol and refluxed for 18 hours. The reaction mixture is evaporated under reduced pressure and dried at high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858781B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-13bffc3b02714c728eadcbf371d025a7 |
| Source note | uspto-grants-2010_12 |