1,1-Dimethylhydrazine → HCID 18606553, compound

HRID 2267700Notes

Reaction equation

HRID 2267700 reaction equation
[CH3:1][N:2]([CH3:4])[NH2:3].[CH2:5]([N:12]1[CH2:17][CH2:16][C:15](=O)[CH:14]([CH3:19])[CH2:13]1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>C(O)C>[CH2:5]([N:12]1[CH2:17][CH2:16]/[C:15](=[N:3]\[N:2]([CH3:4])[CH3:1])/[CH:14]([CH3:19])[CH2:13]1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 59761,1-DimethylhydrazineHCID 5609651-Benzyl-3-methyl-4-piperidone

Product 1

HCID 18606553HCID 18606553, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

N,N-dimethylhydrazine (3 ml, 39.3 mmol) and 1-benzyl-3-methyl-piperidin-4-one (4 g, 19.7 mmol) are dissolved in 50 ml of ethanol and refluxed for 18 hours. The reaction mixture is evaporated under reduced pressure and dried at high vacuum.

Workup

  1. temperaturerefluxed for 18 hours
  2. customThe reaction mixture is evaporated under reduced pressure
  3. customdried at high vacuum

Sources & evidence

ORD record
ord-13bffc3b02714c728eadcbf371d025a7
Source dataset
uspto-grants-2010_12
Patent number
US07858781B2

Reaction notes

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