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HRID2267710

反应详情

EQUATION

反应方程式

HRID 2267710 的结构方程式

REACTANTS

反应物

2
结构：C[C@@H]1CO1
HCID146261

(2R)-2-Methyloxirane

C3H6O

结构：C[C@H]1CNCC[C@@H]1OC(=O)C(C)(C)C
HCID59600241

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H](O)CN1CC[C@H](OC(=O)C(C)(C)C)[C@@H](C)C1
HCID66841391

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

A solution of piperidine 17 (2 g, 10.8 mmol) and (R)-2-Methyl-oxirane (3.78 ml, 54 mmol) in 2 ml of ethanol is stirred for 24 hours in a closed flask. The solvent is evaporated and the residue distilled in a Kugelrohr apparatus (0.08 mbar, 75-90 C).

WORKUP

后处理

  1. customThe solvent is evaporated
  2. distillationthe residue distilled in a Kugelrohr apparatus (0.08 mbar, 75-90 C)