Phthalic Acid → HCID 86625658, compound

HRID 2267953Notes

Reaction equation

HRID 2267953 reaction equation
[CH3:1][N:2]([CH3:5])[CH2:3][CH3:4].[C:6]([OH:17])(=[O:16])[C:7]1[C:8](=[CH:12][CH:13]=[CH:14][CH:15]=1)[C:9]([OH:11])=[O:10]>CO>[CH3:1][NH+:2]([CH3:5])[CH2:3][CH3:4].[C:6]([O-:17])(=[O:16])[C:7]1[C:8](=[CH:12][CH:13]=[CH:14][CH:15]=1)[C:9]([O-:11])=[O:10]

Participants

4

Reactant 2

HCID 1017Phthalic AcidHCID 11723Dimethylethylamine

Product 1

HCID 86625658HCID 86625658, compoundYield 98%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Further, dimethylethylamine (0.1 mol) was added into a methanol solution of phthalic acid (0.1 mol) to obtain a dimethylethylammonium• phthalate solution. Then, said solution was distilled while being heated at 110° C. under reduced pressure of 1.0 KPa or lower to remove methanol, thereby obtaining dimethylethylammonium• phthalate. The yield was 98%.

Sources & evidence

ORD record
ord-d9d58fbc8cf04ffeb087a8a922278968
Source dataset
uspto-grants-2010_12
Patent number
US07859828B2

Reaction notes

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