HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Acid → HCID 86625658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Acid | HCID 1017 | — |
| Reactant | Dimethylethylamine | HCID 11723 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86625658 | HCID 86625658 | 98% |
Reaction Steps
Further, dimethylethylamine (0.1 mol) was added into a methanol solution of phthalic acid (0.1 mol) to obtain a dimethylethylammonium• phthalate solution. Then, said solution was distilled while being heated at 110° C. under reduced pressure of 1.0 KPa or lower to remove methanol, thereby obtaining dimethylethylammonium• phthalate. The yield was 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07859828B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-d9d58fbc8cf04ffeb087a8a922278968 |
| Source note | uspto-grants-2010_12 |