HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-6-iodohexane → HCID 18348353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-6-iodohexane | HCID 67733 | — |
| Reactant | 1-Fluoro-3-iodobenzene | HCID 70725 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 18348353 | HCID 18348353 | — |
Reaction Steps
1-Fluoro-3-(perfluorohexyl) benzene was prepared by heating 6.02 g 1-fluoro-3-iodobenzene and 13.3 g perfluorohexyl iodide with excess copper in dimethyl sulfoxide (DMSO) at approximately 125° C. for 24 hours. The product, 1 -fluoro-3-perfluorohexyl benzene, was obtained in good yield (10.0 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326337B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-3abea3afc416420095381ffd05033d0e |
| Source note | uspto-grants-2001_12 |