HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → Methyl 4-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloylamino]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | 3-(5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride | HCID 73431556 | — |
| Product | Methyl 4-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloylamino]benzoate | HCID 70214611 | — |
Reaction Steps
In a similar manner to that of Example 1(d), by reaction of 1.5 g (10 mmol) of methyl 4-amino-benzoate with 2.8 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride, 3.2 g (82%) of the expected methyl ester are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326510B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-eb9e98d0e30a47f78b987a0381e84a2a |
| Source note | uspto-grants-2001_12 |