HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 4-Hydroxybenzoate → Benzyl 4-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyloxy]-benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 4-Hydroxybenzoate | HCID 7180 | — |
| Reactant | 3-(5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride | HCID 73431556 | — |
| Product | Benzyl 4-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyloxy]-benzoate | HCID 70215804 | — |
Reaction Steps
In a similar manner to that of Example 1 (d), by reaction of 2.3 g (10 mmol) of benzyl 4-hydroxy-benzoate with 2.8 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride, 1.7 g (37%) of the expected benzyl ester, with a melting point 97-9° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326510B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-e993d2a7ed5d48178029310f3b843c79 |
| Source note | uspto-grants-2001_12 |