Thionyl Chloride → HCID 73431553, compound

HRID 2268209Notes

Reaction equation

HRID 2268209 reaction equation
[CH3:1][C:2]1([CH3:20])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6]([C:14]([CH3:19])=[CH:15][C:16](O)=[O:17])[CH:5]=[CH:4][C:3]1=2.S(Cl)([Cl:23])=O>>[CH3:1][C:2]1([CH3:20])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6]([C:14]([CH3:19])=[CH:15][C:16]([Cl:23])=[O:17])[CH:5]=[CH:4][C:3]1=2

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 54560254HCID 54560254, compound

Product 1

HCID 73431553HCID 73431553, compound

Procedure

In a similar manner to that of Example 1(c), by reaction of 2.7 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-butenoic acid with 800 μl of thionyl chloride, 2.9 g (100%) of the expected acid chloride are obtained, which product will be used subsequently in the synthesis without further purification.

Workup

  1. customare obtained
  2. customwhich product will be used subsequently in the synthesis without further purification

Sources & evidence

ORD record
ord-0eebdf21b39741d9b5cb7d383a3465d6
Source dataset
uspto-grants-2001_12
Patent number
US06326510B1

Reaction notes

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