HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 73431553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54560254 | HCID 54560254 | — |
| Product | HCID 73431553 | HCID 73431553 | — |
Reaction Steps
In a similar manner to that of Example 1(c), by reaction of 2.7 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-butenoic acid with 800 μl of thionyl chloride, 2.9 g (100%) of the expected acid chloride are obtained, which product will be used subsequently in the synthesis without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326510B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-0eebdf21b39741d9b5cb7d383a3465d6 |
| Source note | uspto-grants-2001_12 |