HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 18349671, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | HCID 52988777 | HCID 52988777 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18349671 | HCID 18349671 | — |
Reaction Steps
1-(4-Benzyloxyphenyl)-1-methylethylamine hydrochloride (25.0 g) was treated with acryloyl chloride (8.43 ml) in dichloromethane (250 ml) containing triethylamine (14.4 ml) to give N-[1-(4-benzyloxyphenyl)-1-methylethyl]acrylamide, m.p. 116-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326500B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-805909f30866455794390e1a6b71a1cd |
| Source note | uspto-grants-2001_12 |