HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22644926, compound → HCID 86757633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22644926 | HCID 22644926 | — |
| Reactant | HCID 86757634 | HCID 86757634 | — |
| Product | HCID 86757633 | HCID 86757633 | 63.5% |
Reaction Steps
(1R,2S)-2-[{[4-(2-Butynyloxy)phenyl]sulfonyl}aminocyclopentanecarboxylic acid (0.506 g, 1.5 mmol) was converted to (1R, 2S)-2-[{[4-(2-butynyloxy)phenyl]sulfonyl}amino)-N-hydroxycyclopentanecarboxamide (0.28 g) as described in Example 21 to give an off-white solid (0.185 g), mp 140-145° C. Electrospray Mass Spec 353.4 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326516B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-3a5661ef03b64648bbf2fc24b1d54446 |
| Source note | uspto-grants-2001_12 |