HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59975285, compound → HCID 59975296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59975285 | HCID 59975285 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | HCID 59975296 | HCID 59975296 | 78.8% |
Reaction Steps
The title compound was prepared by a similar method to example 20 using N-({9-[(2R,3R,4S,5R)-3,4-dihydroxy-5-(methoxymethyl)tetrahydro-2-furanyl]-6-[(2,2-diphenylethyl)amino]-9H-purin-2-yl}methyl)-4-[1-(2,2,2-trfluoroacetyl)-4-piperidinyl]benzenesulfonamide (0.26 g, 0.32 mmol) (example 21) and a saturated methanolic solution of ammonia (20 ml). This gave the title compound (180 mg) as a solid. MS: 715 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326359B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-bf93511599634a0da4ded4f08460fdaa |
| Source note | uspto-grants-2001_12 |