HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18348527, compound → HCID 18348610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18348527 | HCID 18348527 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18348610 | HCID 18348610 | 99.5% |
Reaction Steps
An ethanol (6.0 ml) suspension of ethyl 8-(4,5,6,7-tetramethoxyinden-2-yl)octanoate (310 mg, 0.763 mmols)and 10% palladium-carbon (60 mg) was stirred under a hydrogen atmosphere at room temperature for 4 hours. The palladium-carbon was removed by filtration, and the filtrate was concentrated in vacuo to obtain the entitled compound (310 mg) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326369B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-646416b4118c44639580e44fdaa6342d |
| Source note | uspto-grants-2001_12 |