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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2268637Generated: October 30, 2026

HCID 69948689, compound → HCID 18348847, compound

https://huagongshe.com/reaction/2268637

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69948689HCID 69948689—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 18348847HCID 18348847183.8%

Reaction Steps

A solution of (2-{3-chloro-5-[cyclopentyl-(3-pyrrolidin-1-yl-propyl)-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester trifluoroacetate (0.080 g) in a mixture of dichloromethane (1 ml) and trifluoroacetic acid (1 ml) was stored at room temperature for 2 h and then concentrated under reduced pressure to give the title compound (0.075 g) as a colourless gum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06326386B1
Source datasetuspto-grants-2001_12
ORD IDord-f8da31327ad94f108e1de4cad5a2ba49
Source noteuspto-grants-2001_12