HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18348884, compound → HCID 18348976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18348884 | HCID 18348884 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18348976 | HCID 18348976 | 734.7% |
Reaction Steps
A solution of 4-({3-[2-(tert-butoxycarbonyl-pyridin-4-yl-amino)-ethoxy]-5-chloro-benzoyl}-cyclopentyl-amino)-butyric acid (0.015 g) in trifluoroacetic acid (3 ml) was stored at room temperature for 2 h and then the solvent removed under reduced pressure. The residue was purified by preparative hplc to give title compound (0.09 g) as a colourless gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326386B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-4e02574ddec643e4b4c98c41ffefb927 |
| Source note | uspto-grants-2001_12 |