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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2268663Generated: October 30, 2026

HCID 69947962, compound → HCID 18349009, compound

https://huagongshe.com/reaction/2268663

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69947962HCID 69947962—
SolventDichloromethaneHCID 6344—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 18349009HCID 1834900984.1%

Reaction Steps

A solution of (2-{3-chloro-5-[(2-diethylcarbamoyl-ethyl)-isopropyl-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester trifluoroacetate (0.06 g) in a mixture of dichloromethane (2 ml) and trifluoroacetic acid (1 ml) was stored at room temperature for 3 h and then concentrated under reduced pressure to give the title compound as a colourless oil (0.043 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06326386B1
Source datasetuspto-grants-2001_12
ORD IDord-9984bab9da454b3bb1b29c4ba83df6a5
Source noteuspto-grants-2001_12