HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69947962, compound → HCID 18349009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69947962 | HCID 69947962 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18349009 | HCID 18349009 | 84.1% |
Reaction Steps
A solution of (2-{3-chloro-5-[(2-diethylcarbamoyl-ethyl)-isopropyl-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester trifluoroacetate (0.06 g) in a mixture of dichloromethane (2 ml) and trifluoroacetic acid (1 ml) was stored at room temperature for 3 h and then concentrated under reduced pressure to give the title compound as a colourless oil (0.043 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326386B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-9984bab9da454b3bb1b29c4ba83df6a5 |
| Source note | uspto-grants-2001_12 |