HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18349146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 54163406 | HCID 54163406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18349146 | HCID 18349146 | — |
Reaction Steps
A solution of (2-{3-chloro-5-[cyclopentyl-(3-trifluoromethanesulfonylamino-propyl)-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester (0.0118 g) in dichloromethane (1 ml) and trifluoroacetic acid (1 ml) was stored at room temperature for 19 h and then concentrated under reduced pressure. The title compound was obtained as a pale brown gum (0.010 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326386B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-a8639c5bb4c6453e88004b2da8dfdc20 |
| Source note | uspto-grants-2001_12 |