HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18349164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69949759 | HCID 69949759 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18349164 | HCID 18349164 | — |
Reaction Steps
A solution of {2-[3-chloro-5-(phenyl-2-(pyridin-2-yloxy)-ethyl-carbamoyl)-phenoxy]-ethyl}-pyridin-4-yl-carbamic acid tert-butyl ester (0.065 g) and trifluoroacetic acid (0.75 ml) in dichloromethane (0.75 ml) was stirred at room temperature for 2 h then concentrated under vacuum, co-evaporating with dichloromethane to give the title compound as a yellow oil (0.086 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326386B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-be0cc362416d45cab7f8c1e5f2600cdd |
| Source note | uspto-grants-2001_12 |