Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2268686Generated: October 30, 2026

Trifluoroacetic acid → HCID 18348872, compound

https://huagongshe.com/reaction/2268686

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 69949518HCID 69949518—
SolventDichloromethaneHCID 6344—
ProductHCID 18348872HCID 18348872—

Reaction Steps

A solution of (2-{3-chloro-5-[isopropyl-(2-sulfamoyl-ethyl)-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester (0.012 g) in a mixture of dichloromethane (1 ml) and trifluoroacetic acid (1 ml) was stored at room temperature for 64 h and then concentrated under reduced pressure to give the title compound (0.011 g) as a colourless gum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06326386B1
Source datasetuspto-grants-2001_12
ORD IDord-d178157feb234444a0d9233125df7dd5
Source noteuspto-grants-2001_12