Acetonitrile → HCID 131723008, compound

Participants

Reaction Steps

Chinolin (5.2 g, 40 mmol) and 6-bromo-hexanicacid (7.8 g, 40 mmol) was added to 30 ml acetonitrile. The mixture was refluxed under nitrogen atmosphere for three hours and then stirred for 15 hours at room temperature. 50 ml acetone was added and the solution was stirred for further 1 hour. The white precipitate was filtered, washed with acetone (2*10 ml) and dried.

Provenance & Evidence