Potassium Bromide → HCID 178433127, compound

Participants

Reaction Steps

was prepared according to procedure used for (2) in Example 1; yield 5%. mp: >300° C. (DMF). IR (KBr): υ=2878, 1748. 1700, 1625, 1557, 1474, 1357, 1219, 744 cm−1. 1H-NMR (CF3CO2D): δ=2.64 (s, 3H, CH3), 3.88 (s, 2H, CH2), 7.52 (m, 2H, 2×Harom), 7.67 (m, 2H, 2×Harom). Accurate mass: calculated: 299.1018. Found 299.1013. Analysis calculated for C14H13N5O3: C, 55.2; H, 4.40; N, 23.40. Found: C. 55.4; H, 4.7; N, 22.5.

Provenance & Evidence