HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178494228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 11098103 | HCID 11098103 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178494228 | HCID 178494228 | 75.3% |
Reaction Steps
6-Amino-9-benzyl-2,8-dimethoxypurine (53 mg, 0.186 mmol) in concentrated hydrochloric acid (10 ml) was stirred for 3 hours at room temperature. The reaction mixture was made basic with 28% aqueous ammonia, and the resulting crystals were filtered and washed with water to give the subject compound (38 mg, yield 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-e61945571e634f72ad131f99685d4f4b |
| Source note | uspto-grants-2001_12 |