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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2269019Generated: October 30, 2026

Ammonia → HCID 178467447, compound

https://huagongshe.com/reaction/2269019

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 11130326HCID 11130326—
SolventHydrochloric AcidHCID 313—
ProductHCID 178467447HCID 17846744764.3%

Reaction Steps

6-Amino-9-benzyl-2-ethoxy-8-methoxypurine (18 mg, 0.06 mmol) in concentrated hydrochloric acid (5 ml) was stirred for 3 hours at room temperature. The reaction mixture was made basic with 28% aqueous ammonia, and the resulting crystals were filtered and washed with water to give the subject compound (11 mg, yield 64%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06329381B1
Source datasetuspto-grants-2001_12
ORD IDord-fb05f4a79bd14d80bcdc4d5fa52a7ad3
Source noteuspto-grants-2001_12