HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178495892, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 18332727 | HCID 18332727 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178495892 | HCID 178495892 | 73% |
Reaction Steps
6-Amino-9-benzyl-8-methoxy-2-(2-methoxyethyl)aminopurine (26 mg, 0.079 mmol) in concentrated hydrochloric acid (20 ml) was stirred at room temperature for 7 hours. The reaction mixture was made basic with 28% aqueous ammonia. The resulting crystals were filtered to give the subject compound (18 mg, yield 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-05315196605f4779800948249c9a06d2 |
| Source note | uspto-grants-2001_12 |