HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurine → HCID 178508972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurine | HCID 18332724 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178508972 | HCID 178508972 | 73.2% |
Reaction Steps
6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurine (114 mg, 0.332 mmol) in concentrated hydrochloric acid (20 ml) was stirred at room temperature for 12 hours. The reaction mixture was evaporated in vacuo to dryness and to the residue was added aqueous ammonia. The resulting crystals were filtered to give the subject compound (80 mg, yield 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-dfc27cf75b974098aca2c753192da13c |
| Source note | uspto-grants-2001_12 |