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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2269069Generated: November 1, 2026

6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurine → HCID 178508972, compound

https://huagongshe.com/reaction/2269069

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurineHCID 18332724—
SolventHydrochloric AcidHCID 313—
ProductHCID 178508972HCID 17850897273.2%

Reaction Steps

6-Amino-9-benzyl-2-(4-hydroxybutoxy)-8-methoxypurine (114 mg, 0.332 mmol) in concentrated hydrochloric acid (20 ml) was stirred at room temperature for 12 hours. The reaction mixture was evaporated in vacuo to dryness and to the residue was added aqueous ammonia. The resulting crystals were filtered to give the subject compound (80 mg, yield 73%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06329381B1
Source datasetuspto-grants-2001_12
ORD IDord-dfc27cf75b974098aca2c753192da13c
Source noteuspto-grants-2001_12