HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-9-benzyl-8-methoxy-2-(2-methoxyethoxy)purine → HCID 178496186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-9-benzyl-8-methoxy-2-(2-methoxyethoxy)purine | HCID 11278904 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178496186 | HCID 178496186 | 84.2% |
Reaction Steps
6-Amino-9-benzyl-8-methoxy-2-(2-methoxyethoxy)purine (21 mg, 0.064 mmol) in concentrated hydrochloric acid (20 ml) was stirred at room temperature for 5 hours. The reaction mixture was evaporated in vacuo to dryness and 28% aqueous ammonia was added to the residue. The resulting crystals were filtered and washed with water to give the subject compound (17 mg, yield 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-12280cda89df4007be713dc0890864f8 |
| Source note | uspto-grants-2001_12 |