HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18347065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18347140 | HCID 18347140 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18347065 | HCID 18347065 | 81% |
Reaction Steps
In a similar manner to that described in Example (1b), a solution of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-(3,3-diphenylpropyl)amine (3.53 g) [prepared as described in step (a) above] in ethanol (70 ml), nickel chloride hexahydrate (3.71 g) and sodium borohydride (1.18 g) were reacted, to afford the title compound (2.67 g) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-e930b556bc5b40dba8e7f3313d2b4214 |
| Source note | uspto-grants-2001_12 |