Sodium borohydride → HCID 18347047, compound

Participants

Reaction Steps

In a similar manner to that described in Example (1b), a solution of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-[1-(3,5-difluorophenyl)ethyl]amine (2.65 g) [prepared as described in step (a) above] in methanol (50 ml), nickel chloride hexahydrate (3.16 g) and sodium borohydride (1.0 g) were reacted, to afford the title compound (2.24 g) as a pale orange oil.

Provenance & Evidence