Sodium borohydride → HCID 70188165, compound

Participants

Reaction Steps

In a similar manner to that described in Example (1b), a solution N-[(3-nitrophenyl)-(4-methoxyphenyl)methyl]-N-[(S)-1-(3-fluorophenyl)ethyl)amine (2.70 g) [prepared as described in step (a) above] in methanol (100 ml), nickel chloride hexahydrate (3.37 g) and sodium borohydride (1.13 g) were reacted, to afford the title compound (2.32 g) as a yellow oil.

Provenance & Evidence