HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70189225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 70188147 | HCID 70188147 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 70189225 | HCID 70189225 | 74.8% |
Reaction Steps
In a similar manner to that described in Example (1b), isomer B of N-[(3-nitrophenyl)-4-pyridylmethyl]-[(S)-1-phenylethyl]amine (1.02 g), nickel chloride hexahydrate (1.47 g) and sodium borohydride (470 mg) were reacted, to afford isomer B of the title compound (694 mg) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-ebe7cd1acf7843e7b0e9102d5e070473 |
| Source note | uspto-grants-2001_12 |