HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334185 | HCID 18334185 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18334157 | HCID 18334157 | 73.3% |
Reaction Steps
In a similar manner to that described in Example (1b), a solution of 2-{[(4-methoxyphenyl)-(3-nitrophenyl)methyl]amino}-1-phenylethanol (3.26 g) [prepared as described in step (b) above] in methanol (60 m), nickel chloride hexahydrate (4.09 g) and sodium borohydride (1.3 g) were reacted, to afford the title compound (2.2 g) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-44fb64fd108d466884b7a62e4c6cce4d |
| Source note | uspto-grants-2001_12 |