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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2269431Generated: November 1, 2026

Sodium borohydride → HCID 18334157, compound

https://huagongshe.com/reaction/2269431

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 18334185HCID 18334185—
CatalystDichloronickel;hexahydrateHCID 11791229—
SolventMethanolHCID 887—
ProductHCID 18334157HCID 1833415773.3%

Reaction Steps

In a similar manner to that described in Example (1b), a solution of 2-{[(4-methoxyphenyl)-(3-nitrophenyl)methyl]amino}-1-phenylethanol (3.26 g) [prepared as described in step (b) above] in methanol (60 m), nickel chloride hexahydrate (4.09 g) and sodium borohydride (1.3 g) were reacted, to afford the title compound (2.2 g) as a yellow oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06329405B1
Source datasetuspto-grants-2001_12
ORD IDord-44fb64fd108d466884b7a62e4c6cce4d
Source noteuspto-grants-2001_12