HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 18347088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 18347118 | HCID 18347118 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18347088 | HCID 18347088 | — |
Reaction Steps
In a similar manner to that described in Example (1d), 3-methoxy-4-{3-[(4-methoxyphenyl)-(2-cyclohexylethylamino)methyl]phenylamino}-3-cyclobutene-1,2-dione (630 mg) [prepared as described in step (c) above] and a solution of ammonia in ethanol (2N, 2.8 ml) were reacted, to give the title compound (536 mg) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-70e4fef387ce4fb4b7692f32697139f1 |
| Source note | uspto-grants-2001_12 |