HRID2269445
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Following a similar procedure to that described in Example (1b), 870 mg of N-[1-(3,5-difluorophenyl)ethyl-N-[(3,4-dimethoxy-5-nitrophenyl)-(4-methoxyphenyl)methyl]amine [prepared as described in step (a) above], 1.04 g of nickel chloride hexahydrate and 302 mg of sodium borohydride were reacted, to obtain 550 mg of the title compound as a colorless oil.
WORKUP
后处理
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